Describes a method based on prior conversion of the sulphur compounds in a test portion to sulphate, if required, and reduction of the sulphate ions ti hydrogen sulphide by a mixture of hydriodic and phosphinic acids in the presence of hydrochloric acid. The hydrogen sulphide is entrained in a current of nitrogen and absorbed in a solution of sodium hydroxide in aqueous acetone, followed by titration of the sulphide ions with standard volumetric mercury(II) acetate or nitrate solution in the presence of 1,5-diphenyl-3-thiocarbazone (dithiozone) as indicator.
Document identifier
ISO 6228:1980
Title
Chemical products for industrial use -- General method for determination of traces of sulphur compounds, as sulphate, by reduction and titrimetry
ISO Category
TC 47/SC 1: General methods
Publication date
1980-11-01
International Relationship
BS 6337-1:1983
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